Fundamental Chemical Experiments-E2

Numbering Code U-LAS13 10012 EE60 Year/Term 2022 ・ Second semester
Number of Credits 2 Course Type Experiment
Target Year Mainly 1st year students Target Student For science students
Language English Day/Period Wed.3・4/Fri.3・4
Instructor name Juha Lintuluoto (Graduate School of Engineering Associate Professor)
ALCANTARA AVILA, Jesus Rafael (Graduate School of Engineering Senior Lecturer)
Nguyen Thanh Phuc (Graduate School of Engineering Senior Lecturer)
Cedric Tassel (Graduate School of Engineering Associate Professor)
LANDENBERGER, Kira Beth (Graduate School of Engineering Senior Lecturer)
Yi Wei (Graduate School of Engineering Associate Professor)
(Graduate School of Human and Environmental Studies)
Outline and Purpose of the Course The purpose of this laboratory class is to practice the basic identification and synthesis of chemical compounds as well as to learn the underlying principles involved.
Course Goals Students will gain understanding in basic chemical concepts by actual hands-on work performing fundamental analysis of chemical compounds.
Schedule and Contents Registration information: https://www.z.k.kyoto-u.ac.jp/zenkyo/guidance

1. General Guidance [2 times]
The aims and contents of the experiments, how to make laboratory notes and reports, and how to use experimental instruments, labware and reagents safely.

2. Qualitative Inorganic Analysis Experiments [4 times]
(1) Basic Reactions of Fe3+ and Al3+ (3rd Analytical Group).
(2) Basic Reactions of Ag+, Pb+, Cu2+ and Bi3+ (1st and 2nd Analytical Groups).
(3) Basic Reactions of Ni2+, Co2+, Mn2+ and Zn2+ (4th Analytical Group).
(4) Analysis of an Unknown Sample Containing Some Cations.

3. Volumetric Analysis Experiments [4 times]
(1) Chelatometric Titration: Quantitative Determinations of Ca2+ and Mg2+ in tap water.
(2) Iodometry: Quantitative Determination of NaClO in Bleach.
(3) Oxidation Reaction Rate: Measurement of a Pseudo-first-order Reaction Rate Constant.
(4) Adsorption of Oxalic Acid by Activated Carbon.

4. Experiments in Organic Chemistry [4 times]
(1) Qualitative Analysis of Organic Compounds.
(2) Structure and Property of Organic Compounds: Azo Dyes and Fluorescent Dyes.
(3) Organic Synthesis I: Acetylation of 4-Methoxyaniline.
(4) Organic Synthesis II: Nitration and Hydrolysis.

5. Feedback [1 time]
Evaluation Methods and Policy Grades will be based on submitted reports and performance during of a total of 12 hands-on chemical experiments.
Course Requirements None
Study outside of Class (preparation and review) Preparation for each experiment should be done in advance. Understand the principles involved, and summarize these beforehand in the experimental notes regarding the reagents, equipment, and procedures and methods to be used.
Textbooks Textbooks/References Fundamental Chemical Experiments, This textbook will be delivered at the class.
Related URL https://ocw.kyoto-u.ac.jp/en/ilas/02
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