Instrumental Analysis,Adv.I
| Numbering Code |
G-ENG15 5D043 SJ60 G-ENG14 7D043 SJ61 G-ENG13 8D043 SJ61 G-ENG17 8D043 SJ76 |
Year/Term | 2022 ・ First semester | |
|---|---|---|---|---|
| Number of Credits | 1 | Course Type | Seminar | |
| Target Year | Target Student | |||
| Language | Japanese | Day/Period | Thu.4・5 | |
| Instructor name | OOE KOUICHI (Graduate School of Engineering Professor) | |||
| Outline and Purpose of the Course | This postgraduate subject is aimed at students of the six chemistry majors offered by the Graduate School of Engineering. In this subject, lectures and practical training are provided in a relay format by the instructors in charge and TAs. The main purpose of this subject is to help students in postgraduate master's and doctoral programs acquire advanced scientific skills in instrumental analysis through lectures explaining principles of three advanced forms of instrumental analysis, and by offering practical training. In this subject, students take lectures on each instrument to acquire knowledge of analytic principles and methods. Following this, students receive basic and applied training for each instrument. In addition, students are asked to select two of three instruments, then take lectures on them before receiving practical training. | |||
| Course Goals | Through lectures and practical training, the subject ultimately aims to teach students about analysis methods involving the use of advanced scientific instruments, and to improve their analytical accuracy as a tool with which they can analyze new substances and scientific phenomena in individual research. | |||
| Schedule and Contents |
Detailed discussion on advanced instrumental analysis (1 session) X-ray photoelectron spectroscopy, Auger electron spectroscopy, ion scattering spectroscopy, secondary ion mass spectrometry, and LEED are discussed. Detailed discussion on advanced instrumental analysis (1 session) The structure and usage method of the comprehensive surface analyzer (X-ray photoelectron spectrometer) are discussed. Detailed discussion on advanced instrumental analysis (1 session) How to use an X-ray powder diffractometer to conduct qualitative and quantitative analyses on solid powder is discussed. Detailed discussion on advanced instrumental analysis (1 session) The crystallite size-measuring method for metal oxide nanocrystals and the Rietveld refinement method for metal composite oxides are discussed. Detailed discussion on advanced instrumental analysis (1 session) The measurement principles of MALDI-TOF MS are discussed. Detailed discussion on advanced instrumental analysis (1 session) Types of organic matrices and their scope of application, sampling methods, and methods of analyzing data are discussed. Practical training involving the use of instruments [training for basic tasks] (2 sessions) Students engage in practical training for tasks assigned by the instructor- in-charge. Practical training involving the use of instruments [training for applied tasks] (2 sessions) Students engage in practical training for tasks assigned by the instructor-in-charge. |
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| Evaluation Methods and Policy | Students are evaluated based on reports and assignments given on practical training. | |||
| Course Requirements | Students must have already taken “Physical Chemistry,” “Organic Chemistry,” “Inorganic Chemistry,” and “Analytical Chemistry” at the undergraduate level. | |||
| Study outside of Class (preparation and review) | Contact us if necessary. | |||
| Textbooks | Textbooks/References | Distribute materials to be used based on the content of lectures | ||
| References, etc. | Others | |||
